Details
methyl 3-chlorosulfonylbenzoate GMP Manufacturer Global Trade 63555-50-0 with Fast Delivery
- Molecular Formula: C8H7 Cl O4 S
- Molecular Weight: 234.66
- Boiling Point: 345.6±25.0 °C(Predicted)
- PSA： 68.82000
- Density: 1.431
- LogP: 2.48150
methyl 3-chlorosulfonylbenzoate(Cas 63555-50-0) Usage
InChI:InChI=1S/C8H7ClO4S/c1-13-8(10)6-3-2-4-7(5-6)14(9,11)12/h2-5H,1H3
63555-50-0 Relevant articles
SULFONIMIDAMIDE COMPOUNDS AND COMPOSITIONS FOR TREATING CONDITIONS ASSOCIATED WITH NLRP ACTIVITY
-
Page/Page column 508, (2020/08/13)
In one aspect, compounds of Formula AA, ...
Discovery of Selective Inhibitors of Endoplasmic Reticulum Aminopeptidase 1
Maben, Zachary,Arya, Richa,Rane, Digamber,An, W. Frank,Metkar, Shailesh,Hickey, Marc,Bender, Samantha,Ali, Akbar,Nguyen, Tina T.,Evnouchidou, Irini,Schilling, Roger,Stratikos, Efstratios,Golden, Jennifer,Stern, Lawrence J.
, p. 103 - 121 (2020/02/20)
ERAP1 is an endoplasmic reticulum-reside...
Aryl uracil compound or agriculturally acceptable salt and preparation method thereof and herbicide composition
-
Paragraph 0121; 0125; 0127; 0128, (2019/02/03)
The invention provides an aryl uracil co...
Discovery of trans-3-(pyridin-3-yl)acrylamide-derived sulfamides as potent nicotinamide phosphoribosyltransferase (NAMPT) inhibitors for the potential treatment of cancer
Zhang, Kuojun,Ni, Yong,Chen, Jiaxuan,Tu, Zhengchao,Wu, Xiaoxing,Chen, Dong,Yao, Hequan,Jiang, Sheng
, p. 1502 - 1506 (2019/04/17)
Nicotinamide phosphoribosyltransferase (...
63555-50-0 Process route
-
-
67-56-1
methanol
-
-
4052-92-0
3-chlorosulfonylbenzoyl dichloride
-
-
63555-50-0
methyl 3-chlorosulfonylbenzoate
| Conditions | Yield |
|---|---|
|
In
tetrahydrofuran;
at 20 ℃;
for 13h;
|
100%
|
|
pyridine;
In
dichloromethane;
at 20 ℃;
for 2h;
|
92%
|
|
With
pyridine;
In
dichloromethane;
at 10 - 35 ℃;
for 2h;
|
92%
|
|
|
|
|
at -5 ℃;
for 2h;
|
|
|
at 20 ℃;
for 0.416667h;
Cooling with ice;
|
|
|
With
triethylamine;
at 0 - 20 ℃;
|
|
|
In
tetrahydrofuran;
at 20 ℃;
for 10h;
|
2.45 g
|
-
-
4518-10-9
Methyl 3-aminobenzoate
-
-
63555-50-0
methyl 3-chlorosulfonylbenzoate
| Conditions | Yield |
|---|---|
|
Methyl 3-aminobenzoate;
With
tris(bipyridine)ruthenium(II) dichloride hexahydrate; isopentyl nitrite;
In
acetonitrile;
at 20 ℃;
for 0.0833333h;
Sealed tube;
With
thionyl chloride;
In
water; acetonitrile;
at 20 ℃;
for 20h;
Irradiation;
|
76%
|
|
Methyl 3-aminobenzoate;
With
hydrogenchloride; acetic acid; sodium nitrite;
In
water;
at -10 - -5 ℃;
for 1.5h;
With
sulfur dioxide; copper(l) chloride;
In
water; acetic acid;
at 5 - 15 ℃;
for 1h;
|
67%
|
|
Methyl 3-aminobenzoate;
With
hydrogenchloride; sodium nitrite;
In
water;
at 0 ℃;
With
sulfur dioxide; acetic acid; copper(l) chloride;
In
water;
at 20 ℃;
for 3h;
|
42%
|
|
Methyl 3-aminobenzoate;
With
hydrogenchloride; sodium nitrite;
In
water;
at 0 ℃;
for 0.666667h;
With
sulfur dioxide; acetic acid; copper dichloride;
In
water;
at 0 - 20 ℃;
for 0.666667h;
|
63555-50-0 Upstream products
-
67-56-1
methanol
-
4052-92-0
3-chlorosulfonylbenzoyl dichloride
-
186581-53-3
diazomethane
-
4025-64-3
3-Carboxybenzenesulfonyl chloride
63555-50-0 Downstream products
-
111711-77-4
3-(2-Ethoxy-5-oxo-pyrrolidine-1-sulfonyl)-benzoic acid methyl ester
-
854748-13-3
methyl 3-{[{(2R,3S)-2-hydroxy-3-[((2S)-3-methyl-2-{3-[(2-methyl-1,3-thiazol-4-yl)methyl]-2-oxo-1-imidazolidinyl}butanoyl)amino]-4-phenylbutyl}(isobutyl)amino]sulfonyl}benzoate
-
926291-90-9
3-methoxycarbonylbenzenesulfohydrazide
-
926292-02-6
4-cetyloxy-3-methoxybenzophenone-(Z)-3-methoxycarbonylphenylsulfohydrazone
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